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Phil Hamling 376 County Route 1 Warwick, NY, USA 10990 e-mail: pdah-at-optonline.net (change the -at- to @)
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Zinc Silicate Crystalline Glaze Pottery A chronicle of my recent progress and a way for me to keep it straight in my head! Click on thumbnails to enlarge photos |
Info I've been asked to keep in confidence. |
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September 7, 2008
80th Firing Result - WTF????? I thought this was going to a rather mundane firing. It didn't turn out that way. I had a re-fire, 2 pieces with NFU at a low loading (~.35 g / sq. in.) and one piece with NFU + 1/2% cobalt carbonate, which should have yielded pieces with 1 1/2" to 2" dia. crystals. When I first peeked in I saw very few smallish crystals - not what I was expecting. It looked like an overfiring condition, but I have limited experience.
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After closer examination I saw that ^11 had slumped well beyond where it had in the past (^11 touching). The first photo above shows ^'s 9, 10 & 11 from this firing in front and typical cones from previous firings in the rear. It looks more like ^13 to ^14 to me.
I'm in a quandry as to what to do to get back to the normal ^11 touching situation I've seen in the past. I checked the program and saw that nothing had changed. Is it a thermocouple degradation thing? Are they in need of replacement? I would expect platinum Rhodium thermocouples to last a very long time at this temperature. Is it just a "computer thing" and will rebooting the unit set it straight? I have many more pieces I was going to put this this routine firing, but don't want to screw them up and am not quite sure what to do.
Doll Test Firing Result - Well there certainly is some green showing but the pieces are all fish scaled. Even with a 30 minute hold at 1290ºC ^11 only came down to ~3 o'clock. I added another layer of uncolored 8% titania glaze to the pieces when they were still above 100ºC (it sticks prettty well) and refired it with a 35 minutes soak at the top end.
September 6, 2008
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80th Firing Setup |
Doll Test Firing |
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A few more NFU pieces plus a refire. I'm using the schedule of 4-27-08 except I've sped up the first 3 segments |
2 refires plus a new one. All have some copper in hopes of having some nice stuff to reduce at Bill Schran's. |
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September 4, 2008
September 1, 2008 Labor Day Holiday Weekend
August 30, 2008
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Gettin' glaze catchers together. I'm going to stitch the split prismatic one on the seams with scrap platinum thermocouple wire. (Is that an oxymoron or what?) |
Kat got the itch to throw some pots. | ||
August 26, 2008
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My latest attempt at making something of this form. |
More creations from Andy Boswell |
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These sunflowers have re-seeded themselves for several years now and are in peak bloom. |
Connie's Bunnies |
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August 23, 2008 One more try!
Notes on Bill Schran's show
THE CRYSTALLINE SPECTRUM: A JOURNEY FROM STUDENT TO MASTER
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My current studio mate! |
It was glorious out in the yard today. The sun had that intensity which makes fresh cut grass glow. |
The Grasshopper's new stamp. Nice stuff Nathan! |
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August 20, 2008
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A bit of epoxy added to stand 'er up and I think I'm seeing a pot with a little attitude. |
Straight from the goose that laid the golden egg. Thanks a million Mr. Wizard! |
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August 17, 2008
August 17, 2008
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79th firing setup. Mostly NFU at .35 g/sq. in. loading |
Trying to make a little less of a "Pegleg Pete" this time. |
Kat & Dillon's camouflage paint job on the fountain controls. |
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Increasing the hold time to 30 minutes brought ^11 close to touching, but there's nothing to write home about in terms of the glaze. I added 2 1/2 coats of fresh glaze and am firing them for the third time.
August 16, 2008
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Not much background here. I'm re-firing these now. |
Avi, It survived the bisque and is ready for glaze. |
I increased the Doll's hold time at 1290C to 30 minutes in the hopes of getting ^11 touching in this test firing. Maybe that will help with fewer crystals.
August 13, 2008........Totally Off Topic
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A contractor friend of mine has had a job building a Buddhist Temple recently. Pictured are 2 "doohickeys" he'll be installing soon. |
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August 10, 2008
I have to tell you.....This is probably the most rewarding slab built form I've made yet. I really enjoyed the process and like the shape too. I'm sure it breaks many of the "Art" rules, but who cares. I like it. It's about 18 inches tall and I can't wait to see some nice crystalline rings on it. I plan to use NFU at a low loading rate where I'll see minimal glaze run off and have built a glaze catcher kind of doohickey into the base.
This is the kiln I recently bought from a friend for $120. He bought it off the sidewalk from a guy who was trying to get. Although it has strictly manual control I think it will be useful for use as a reduction torture machine. It looks like it is circa the 1970's to me. I'll have to check with Steve Lewicki to find out if the serial number helps date it. I'll bet its older than the Grasshopper.
The elements are in great shape and look like they have seen heat < 1/2 dozen times. The brick between sections was a little chewed up but I applied some ZIRCAR AX Moldable and CTP-1 Paper between the joints and they look to be sealed up right nice!
August 6, 2008
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Nothing better than a fresh hair cut. |
It's amazing how much the weeping willows have recovered from their June 1st pruning. |
Don't tell anyone but Bella has a foot fetish. |
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Tales from the Pickle Jar
This test involved using the same glaze*, on the same clay, in the same firing at different loading rates. (*OK, it had been aged 6, 23 and 65 days in a jar before I used it.) It appears aging (at least for this time period) makes no difference in the reaction of the glaze, but glaze thickness does not only with the color of the background but with the shape and color of the crystals. Note how little runoff there was from the pots with the lower glaze loadings.
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![]() The background color and shape of the brown crystals change significantly with glaze thickness. |
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August 3, 2008
August 2, 2008
I have used Gorilla glue for years but never read the directions. It says to moisten one surface with water which causes the glue to foam. It works like a charm and makes the glue foam and harden in 4 hours. Being water based it doesn't dissolve the blue foam like Super 77 spray adhesive or other petroleum based material do. I'm going to put a bunch of material together an machine the forms on a CNC router this time.
July 30, 2008 - 77th Firing Results
July 26, 2008 - 77th Firing
| July 29, 2008 |
July 28, 2008 |
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| Sneak Preview -250°C | Setup | ||
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| July 24, 2008 |
July 27, 2008 |
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| The Wizard's Army | Glads | Bella, Bella, Bella! | DT reduction. |
Crystalline Glaze Quiz
Name the 5 frequent Crystalline Glaze Forum visitors who created these.
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July 20, 2008
Fishing this weekend in NY's Thousand Islands
Phil won the bet with the 6#, 32" Northern Pike he took off Scow Island with Singer Castle on Dark Island visible across the shipping channel.
July 16, 2008 76th Firing Results
July 14, 2008 76th Firing Setup
July 13, 2008
The results of the 74th firing were poor (from a visual sense) to say the least. The crystals were quite bland and there was virtually no run off in the catcher. So I quickly loaded some more glaze on the bowl getting the loading up to .40 g/sq.in. On the positive side I did learn that a loading of .25 g of solids per sq. in of area just isn't enough. Also there were many, many pinholes. Then Mr. Turner told me, in an attempt to save electricity $, he bisqued these pieces to ^06 using the "Slow Glaze" cycle which runs much faster than the bisque cycles. My guess is the clay wasn't hot enough long enough to complete its dehydroxylation and off gassing.
July 12, 2008
The 17 1/2" dia. David Turner bowl in this firing has the glaze (NFU) brushed as thin as I could while getting a real even single coat. It worked out to be ~.25 g of solids per sq. in of area. This is about 1/2 the loading of June 16th's firing - a lighter loading than I expected. It is reproducible, and I can add more and keep track of exactly how much I have on as I'm glazing.
I expect this will give a look similar to the results of my 68th firing and will see for sure tonight (7-13-08). I plan to explore loadings in between .25 and .5 g solids per sq. in.
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The kitchen is coming along real nice. We're hoping to pick out the granite counter tops this week. John Welch (www.finekitchenandbath.com) has been doing a fantastic job and is a pleasure to work with, plus I think he's more anal than I am, if that's possible! |
Patti modeling the spring loaded wiffle ball antennae earmuffs I made to add a little comedy to lawn mowing. |
This year's blueberry crop is looking real good! |
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July 5, 2008
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July 4, 2008
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June 29, 2008
June 29, 2008
June 27, 2008
June 24, 2008
David, I'd say tonight's smoking was quite nice indeed. You really pulled out all the rings nicely. I wonder if a little iron would give some yellow highlights?
June 23, 2008
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Shaped with wood putty and then 2 coats of latex paint. |
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Before and after 3X reduction by David Turner. |
June 16, 2008 73rd Firing Results
I'm still trying to get a good handle on the relationship of crystal growth to glaze thickness for this glaze when fired in the low temperature range (860C to 1000C). I brushed one heavy coat of the pudding consistency glaze on each piece with and additional 1 1/2" band on top.
For the 2 pieces in the right photo I measured the amount of glaze I added and estimated their surface area to determine the loading rate. They had 0.51 and 0.46 g solids / sq. in. of surface. All these have the characteristic look of some of the first NFU pieces I made. I can, and will, apply the glaze more thinly (0.4 g / in. sq.) on future pieces to hopefully get back to the "explosive" crystal growth I saw before.
Regarding the 2 pieces in the right photo, the one on the left had the 2 1/2 week old glaze and the one on the right had it from a new batch. I don't think the aged stuff worked as well.
June 15, 2008 Happy Father's Day!
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A 2 1/2 week old "pickle jar" of NFU. |
73rd Firing Setup Thanks for the photos, Kat. |
Another beauty by Glenn & Keith. |
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June 13, 2008
I had the good fortune of spending 4 days with John Mankameyer at his home and studio in Miles City, Montana.
He's located deep in the heart of cattle country! On the trail Lewis and Clark followed when exploring in the early 1800's. Near the site of Custer's Last Stand by the Little Big Horn.
John has been making crystalline glazed porcelain since the mid 1970's. After years of doing the show circuit in Northern California now he's retired and still actively experimenting with these glazes and his unique twist to them. John has a motto posted on his PC which reminds him of his charter (I guess) which reads: "I am trying to do more than make a pot with colored blotches on it"
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| Agate - Inspiration For John's Crystalline Glaze | Select Photos From My Visit |
Fort Keogh Livestock and Range Research Laboratory |
Montana Landscape |
June 7, 2008
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I'm off to spend a week with John Mankameyer. |
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June 5, 2008
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| A fantastic birthday present from Avril Farley. | |||
May 31, 2008 72nd Firing Results
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| 3 types of crystals |
1, 3/4, 1/2, 1/4 & 0% MnO2 in NFU in rear. |
The kitchen is going in the studio. Soon I'll be setup for visitors. |
May 29, 2008 71st Firing Results, 12" Diameter X 14 1/2" Tall
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May 27, 2008
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70th Firing Results |
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71st Firing Setup |
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An all Klinsky event. |
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May 26, 2008
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70th Firing Setup |
One coat of wood filler. | |
David Turner's latest big bowl is on the bottom. It is all NFU except for the inside bottom which is 8% rutile base. The top shelf is all NFU too. I gave the pieces a heavy coat of glaze right around the top lips this time to try and get more of the action I've seen around the bottoms further up the pots. The little guys are on their second firing with a little more glaze.
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On Memorial Day, the flag should be hung at half-staff until noon, when it should be raised to the top of the staff. |
May 25, 2008
May 23, 2008
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Replacing elements. I used the the "B Tank" torch to bend the leads around the posts as well as bend the coils in the corners to get them to lay in the slots. I should have stretched them to about 74" length first to put them in compression a little. I'm sure they'll settle in after the first firing.
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May 20, 2008 69th Firing Results
When I got home from the rock pile last night the kiln was still going through the last holds. It did shut off and was cooling, but by "Pumpkin Time" it was still 500°C. I was able to peek and saw it was not good. The crystals looked nice, but the pot had collapsed. I knew those 2 real wet rings on the outside, when I glazed the inside, were the sign of doom!
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I did check into what capability my controller has, but unfortunately I didn't order the amp check feature. I plan to do a continuity and resistance check before the next firing, but I have to admit I loaded a bisque this morning.
May 19, 2008
At 8:00am this morning the cycle should have been 1/2 way through the 9 hours worth of holds. It hadn't even reached top end of 1290°C yet. The programmer was calling for 1257°C but the chamber temperature was only 1240°C. I added some more insulation to the lid and left for work. Then at 11:00am I returned and saw it had topped out and was at 1143°C on its way down to the first hold at 1000°C. It appears to be 8 hours behind schedule.
May 18, 2008
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| 69th Firing Setup |
Cones 9 (left) thru 11 (right) from the last firing |
The Freshman Formal Dance was Friday. Kat got all dolled up and looked like a beautiful woman. |
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It looks like my elements are about done. I was expecting to see an over firing condition when they got to the point of not having enough "snot" to get there (resistance too high) in the programmed time, resulting in a heck of a lot more heat work happening as it slowly, I mean slowly, crept up to top temperature. It looks to me like they are running out of gas as the furnace hit somewhere between ^12 and ^13. I didn't really pay attention but seem to recall the programmer said this cycle took 32 or 33 hours - about 10 hours longer than it should have.
I decided to fire the 69th anyway and watch it (as much as I could). I turned on the 16 segment feature (see firing schedule of April 27, 2008), pressed the start button about 6pm and noticed at about 9:30pm the programmer was calling for 500° but the chamber temperature was 495°C.
After Dance Party Note: We had about 250+ kids here for a party which ran from ~10:15pm (after the dance) until 3:30am (when I started asking people to leave). It was in the barn, the house, the yard and the Christmas Tree Field. It was like Woodstock. Driving rain all night, and mud all around the bonfire. The kids seemed oblivious too it and I imagine had a great time. I have spoken with no angry parents, neighbors, police or attorneys either.
May 14, 2008 68th Firing Results
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The big one and little one in the front are first fires with one even coat (I'm happy to see) of "thick shake" glaze. A little more glaze on top and I think they would have the exaggerated growth low temperature crystals all over them. I haven't seen these crystals grow this large before. There was very little run off to the catchers, but some. Next trial I will add a little more glaze right around the top.
May 12, 2008
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Two test tiles and four re-fire pots - three of which are going back in. |
More glaze with 4% CMC and thick shake consistency. | |
May 11, 2008
May 10, 2008
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| 67th Firing Setup | Norma's last piece |
Hold Temps |
Minis by Graeme Anderson, down in the land of opals. |
This load is all re-fires. I mixed more NFU with 4% CMC. The thick shake consistency made it easy to apply a reasonable coat which stayed put. There is also a test tile strip with 1, 2, 3, 4 and 5 coats of NFU to see if I can get a clearer picture of the relationship of low temperature crystal growth habit to glaze thickness. There is another with 1, 1 3/4, 2 1/2, 3 1/4 and 4% rutile.
May 8, 2008
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This is the firing schedule for the last firing. Many people have asked about it so I put it on my firing schedules page as well as here.
Jesse Hull wrote "You said, "It seems the thickness of this glaze at these low temperatures has a major impact on whether these crystals will form and grow." If you're going to compare glaze thickness -or anything else for that matter- shouldn't you use similar, if not identical, forms? The form on the left is a far cry from the one on the right... going from nearly flat to nearly vertical within your testing scheme. And the one in the middle has a neck which holds glaze that eventually runs onto the shoulder (replacing the glaze which is lost there), while neither of the others do."
Using identical forms and measured amounts of glaze for a glaze thickness comparison certainly would be a good way to quantify the situation. Maybe besides cutting into the piece to measure the glaze thickness there is an optical method to use.
I think these recent pots are examples of ones with glaze on the thin side and ones which have this type of crystal. My observation about "...the thickness of this glaze at these low temperatures..." is based:
1)
On seeing the pot on the right with broadly separating rings on its top
which formed at temperatures below 1000°C.
And on the shoulder where it is thicker, and the high temperature crystals
(1050°C
to 1080°C)
grow
quickly
there is little separation between the low temperature bands.
2) This glaze appears green when thick and tending towards aqua when thin. This thick - thin is based on believing I know how much I've brushed on.
3)
Seeing these greenish pieces
not having formed crystals at these low temperatures and knowing I brushed
on a very heavy application of glaze.
4) Re-firing the piece, seeing the glaze flow off the pot and accumulate in the catcher, the color change towards aqua and crystals forming.
I
think the piece on the right exhibits a greener color on the bottom where
the glaze is thick and has small crystals with more of a traditional look,
and tends toward aqua color on the top where the glaze is thin and has
larger, faster growing crystals on top where the glaze is thin.
It's interesting to note though that I may say fast or slow, but the "fast" growing ones here in this "thin" glaze at these low temperatures (860°C to 1000°C) only grow at a rate of ~1inch in 9 hours. That should be enough time to grow 6" diameter crystals at higher temperatures (1080°C)
May 7, 2008 66th Firing Results (Probably the lightest load since firing #9)